| Journal: | Quimica nova |
| Database: | PERIÓDICA |
| System number: | 000313431 |
| ISSN: | 0100-4042 |
| Authors: | Feltrin, Carlos Willian1 Mello, Ana Maria de Souza Santos, Joao Gabriel Rosa dos Marques, Marcelo Volpatto Seibel, Nair Maria Fontoura, Luiz Antonio Mazzini |
| Institutions: | 1Fundacao de Ciencia e Tecnologia, Departamento de Quimica, Cachoeirinha, Rio Grande do Sul. Brasil |
| Year: | 2007 |
| Season: | Feb |
| Volumen: | 30 |
| Number: | 1 |
| Pages: | 80-82 |
| Country: | Brasil |
| Language: | Portugués |
| Document type: | Artículo |
| Approach: | Experimental, aplicado |
| English abstract | A method for HPLC determination of sulfadimethoxyne in milk is presented. The analyte isolation and concentration were performed by solid-phase extraction through a C-8 cartridge, pre-conditioned with hexane, methanol and water and eluted with MeOH. The recovery determination was done with a spiked solution of 20, 50 or 100 µg L-1. In this concentration range, the recovery was 83.2% with a RDS of 15.4%. For quantification, a Zorbax Eclipse XDB-C8 (4.6 mm x 150 mm, 5 µm), a mobile phase of MeCN: 0.01 mol L-1 KH2PO4 aq. (1:4), and a variable wavelength detector (275 nm) were used |
| Disciplines: | Química |
| Keyword: | Química de alimentos, Leche, Sulfadimetoxina, Cromatografía líquida de alta resolución (HPLC) |
| Keyword: | Chemistry, Food chemistry, Milk, Sulfadimethoxyne, High performance liquid chromatography (HPLC) |
| Full text: | Texto completo (Ver HTML) |
