| Journal: | Quimica nova |
| Database: | PERIÓDICA |
| System number: | 000313372 |
| ISSN: | 0100-4042 |
| Authors: | Lino, Celeste Matos1 Baeta, Lurdes Pena, Angelina Simões Silveira, Irene Noronha |
| Institutions: | 1Universidade de Coimbra, Faculdade de Farmacia, Coimbra. Portugal |
| Year: | 2006 |
| Season: | Jun |
| Volumen: | 29 |
| Number: | 3 |
| Pages: | 436-439 |
| Country: | Brasil |
| Language: | Inglés |
| Document type: | Artículo |
| Approach: | Experimental |
| English abstract | An analytical study based on extraction with acetonitrile-water, immunoaffinity column cleanup, and HPLC/fluorescence detection for separation and identification of ochratoxin A in coriander was carried out. Validation of the applied methodology was done through accuracy and precision studies. Homogenized samples of coriander were spiked in triplicate with ochratoxin A at 0.5, 1.0, 2.0, and 5.0 µg/kg levels. Recovery values were in the range of 98% for a fortification level at 0.5 µg/kg to 109.1% at 1.0 µg/kg. Application to coriander samples available in Portuguese markes showed no contamination with ochratoxin A |
| Disciplines: | Química |
| Keyword: | Fitoquímica, Ocratoxina A, Cilantro, Cromatografía líquida de alta resolución (HPLC) |
| Keyword: | Chemistry, Phytochemistry, Ochratoxin A, Coriander, High performance liquid chromatography (HPLC) |
| Full text: | Texto completo (Ver HTML) |
