| Journal: | Polimeros (Sao Carlos) |
| Database: | PERIÓDICA |
| System number: | 000314284 |
| ISSN: | 1678-5169 |
| Authors: | Romao, Benedita M.V1 Diniz, Milton F2 Azevedo, Margarete F.P Lourenco, Vera L Pardini, Luiz C Dutra, Rita C.L Burel, Fabrice |
| Institutions: | 1Instituto Tecnologico da Aeronautica, Centro Tecnico Aeroespacial, Sao Jose dos Campos, Sao Paulo. Brasil 2Instituto de Aeronautica e Espaco, Centro Tecnico Aeroespacial, Sao Jose dos Campos, Sao Paulo. Brasil |
| Year: | 2006 |
| Season: | Ene-Mar |
| Volumen: | 16 |
| Number: | 1 |
| Pages: | 94-98 |
| Country: | Brasil |
| Language: | Inglés |
| Document type: | Artículo |
| Approach: | Experimental, aplicado |
| English abstract | Samples of epoxy resin (EP) based on the diglycidyl ether of bisphenol A (DGEBA), cured with nadic methyl anhydride (NMA) and mercaptan (CAPCURE 3-800), or amine-phenol (CAPCURE EH-30), respectively, SE 4 and SE 5, were prepared in the stoichiometric ratio determined by the supplier. The curing behaviour of the epoxy systems SE 4 and SE 5 was followed by DSC (Differential Scanning Calorimetry). These SE and their ingredients were analyzed using FTIR transmission techniques (KBr pellets, pyrolysis without control and controlled pyrolysis-FT-IR, the CONTROLPIR/FT-IR) for characterizing the curing agents (CA). The temperature range used for samples pyrolysis was found from TG (thermogravimetry). Thus, the FT-IR bands of liquid pyrolysate obtained by CONTROLPIR/FT-IR were evaluated, in comparison to the reference spectrum of CA. The characterization of CA was also possible, by the analysis of such SE with the TG/FT-IR technique |
| Disciplines: | Ingeniería |
| Keyword: | Ingeniería de materiales, Ingeniería aeronáutica, Resinas epóxicas, Agentes de cura, Pirólisis |
| Keyword: | Engineering, Materials engineering, Aerospace engineering, Epoxy resins, Curing agents, Pyrolysis |
| Full text: | Texto completo (Ver HTML) |
