Influencia da geometria da plataforma na determinacao de chumbo em zidovudina (AZT) por ET AAS



Título del documento: Influencia da geometria da plataforma na determinacao de chumbo em zidovudina (AZT) por ET AAS
Revue: Quimica nova
Base de datos: PERIÓDICA
Número de sistema: 000199680
ISSN: 0100-4042
Autores: 1


Instituciones: 1Fundacao Oswaldo Cruz, Escola Nacional de Saude Publica, Rio de Janeiro. Brasil
2Fundacao Oswaldo Cruz, Instituto de Tecnologia em Farmacos (Far-Manguinhos), Rio de Janeiro. Brasil
Año:
Periodo: May-Jun
Volumen: 25
Número: 3
Paginación: 379-383
País: Brasil
Idioma: Portugués
Tipo de documento: Artículo
Enfoque: Experimental
Resumen en inglés The aim of this work was to compare the performances of the L'vov and integrated platforms in order to overcome the interferences found on lead determination in zidovudine by ET AAS. Pyrolysis and atomization temperatures found with integrated platform were 700 and 1400°C, respectively. The characteristic masses were 12.7 ± 1.2 pg with integrated platform and 11.1 ± 1.3 pg with grooved platform. The ratio between the slopes of zidovudine and aqueous curves shows a decrease in the interferences when the L'vov platform is used (bAZT/baq = 0.97 ± 0.10) and the detection limit found was 0.03 µg.g-1. That ratio was 0.85 ± 0.07 with the integrated platform
Disciplinas: Medicina,
Química
Palabras clave: Farmacología,
Toxicología,
Química analítica,
Plomo,
Análisis,
Interferencias,
Zidovudina,
Espectrometría,
Geometría de plataforma,
AZT,
Absorción atómica
Keyword: Medicine,
Chemistry,
Pharmacology,
Toxicology,
Analytical chemistry,
Lead,
Analysis,
Interferences,
Zidovudine,
Atomic absorption,
Spectrometry,
Platform geometry
Texte intégral: Texto completo (Ver HTML)