A microwave-heated infrared reaction cell for the in-situ study of heterogeneous catalysts



Título del documento: A microwave-heated infrared reaction cell for the in-situ study of heterogeneous catalysts
Revue: Ciencia (Maracaibo)
Base de datos: PERIÓDICA
Número de sistema: 000323505
ISSN: 1315-2076
Autores: 1
1
1
Instituciones: 1Edinburgh University, School of Chemistry, Edimburgo. Reino Unido
Año:
Volumen: 14
Paginación: 17-25
País: Venezuela
Idioma: Inglés
Tipo de documento: Artículo
Enfoque: Experimental, analítico
Resumen en inglés A transmission infrared microreactor cell which holds a pressed disc in a controlled atmosphere and allows microwave and conventional heating up to 423 K is demonstrated using the oxidation of carbon monoxide over the standard catalyst EUROPT-1. Optical characteristics are determined by the choice of CaF2 as the window material, allowing transmission from 77 000–1000 cm 1. An oscillating microwave power regime with a peak height of 200 W is used and time-resolved infrared spectra and mass spectrometry show oscillations in the reaction which correspond to the microwave heating
Disciplinas: Física y astronomía
Palabras clave: Física de partículas y campos cuánticos,
Microondas,
Catálisis heterogénea,
Celdas,
Infrarrojo
Keyword: Physics and astronomy,
Particle physics and quantum fields,
Microwaves,
Heterogeneous catalysis,
Cells,
Infrared
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