A new ordered vacancy compound; preparation and crystal structure of Ag3In5□Te9



Document title: A new ordered vacancy compound; preparation and crystal structure of Ag3In5□Te9
Journal: Revista mexicana de física
Database: PERIÓDICA
System number: 000438881
ISSN: 0035-001X
Authors: 1
2
3
Institutions: 1Universidad Libre, Facultad de Ingeniería, Bogotá. Colombia
2Instituto Mexicano del Petróleo, Centro de Tecnología para Aguas Profundas, Veracruz. México
3Universidad de Los Andes, Facultad de Ciencias, Mérida. Venezuela
Year:
Season: Sep-Oct
Volumen: 65
Number: 5
Country: México
Language: Inglés
Document type: Artículo
Approach: Analítico, teórico
English abstract The new ordered vacancy compound Ag3In5□Te9 was synthesized by the melt and annealing technique and its structure was refined from X-ray powder diffraction pattern using the Rietveld method. The title compound crystallizes in the tetragonal space group P 4 -2c(N ° 112), with a = 6.3453(2) Å, c = 12.5754(7) Å, V = 506.32(4) Å 3. The refinement of 23 instrumental and structural parameters led to Rp = 5.4%, Rwp = 5.8%, Rexp = 5.1%, S = 1.1. This ternary compound is isostructural with Cu3In5□Te9 and have a defect adamantane structure
Disciplines: Física y astronomía
Keyword: Física de materia condensada,
Compuesto de vacantes ordenado,
Estructura cristalina,
Difracción de rayos X en polvo,
Refinamiento de Rietveld
Keyword: Condensed matter physics,
Ordered vacancy compound,
Crystal structure,
X-ray powder diffraction,
Rietveld refinement
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