Injetor multicanal com valvulas de estrangulamento para analise em fluxo



Document title: Injetor multicanal com valvulas de estrangulamento para analise em fluxo
Journal: Quimica nova
Database: PERIÓDICA
System number: 000198657
ISSN: 0100-4042
Authors: 1


1
Institutions: 1Universidade de Sao Paulo, Instituto de Quimica, Sao Paulo. Brasil
Year:
Season: Sep-Oct
Volumen: 24
Number: 5
Pages: 689-692
Country: Brasil
Language: Portugués
Document type: Artículo
Approach: Experimental, divulgación
English abstract An important component for the automation of flow injection analysis (FIA) systems is the sample injection valve. A simple and inexpensive commutator with 16 pinch valves (8 normally open and 8 closed) was developed and configured as a multichannel injection valve. It is activated by a single solenoid of 3 Kgf, powered by a pulsed driver circuit, controlled by a microcomputer or a switch. FIA with spectrophometric detection of potassium dichromate solution was used for the evaluation of the new injection valve and its comparison with other valves, for sample loops of 50, 100, 200, 300 and 500 mL. The repeatability was favorable (RSD 1.0% for 15 injections at each loop volume) compared to a manual injector, an electropneumatic injector and an injector configured with three mini solenoid valves (RSD 1.1, 1.3 and 1.0%, respectively, for15 injections at each loop volume)
Disciplines: Ingeniería,
Química
Keyword: Equipo y maquinaria,
Química analítica,
Análisis en flujo,
Automatización,
Válvula de inyección,
Análisis de inyección en flujo,
Volumen de carga,
Válvulas
Keyword: Engineering,
Chemistry,
Equipment and machinery,
Analytical chemistry,
Flow analysis,
Automation,
Injection valve,
Flow injection analysis,
Loop volume,
Valves
Full text: Texto completo (Ver HTML)