Synchrotron radiation X-ray multiple diffraction in the study of KDP phase transition induced by electric field



Título del documento: Synchrotron radiation X-ray multiple diffraction in the study of KDP phase transition induced by electric field
Revista: Materials research
Base de datos: PERIÓDICA
Número de sistema: 000312480
ISSN: 1516-1439
Autores: 1



2




3
Instituciones: 1Universidade Estadual de Campinas, Instituto de Fisica "Gleb Wataghin", Campinas, Sao Paulo. Brasil
2Universidade Federal do Ceara, Departamento de Fisica, Fortaleza, Ceara. Brasil
3Universidade de Sao Paulo, Instituto de Fisica, Sao Paulo. Brasil
Año:
Periodo: Ene
Volumen: 4
Número: 1
Paginación: 43-46
País: Brasil
Idioma: Inglés
Tipo de documento: Artículo
Enfoque: Experimental
Resumen en inglés In this work, the application of the X-ray multiple diffraction technique using synchrotron radiation at Laboratório Nacional de Luz Síncrotron (LNLS) to study KDP phase transition induced by electric field is discussed. A Huber three-axis (w, f, 2q) diffractometer mounted on a table which rotates around the incident beam allows to measure Renninger scans (RS) at the XRD station of LNLS using the adequate polarization for the experiments. Prior results indicated (080) as the best choice for the KDP primary reflection and the (440)( 40) four-beam case for the secondary. Two Bragg-surface diffraction (BSD) reflections, where the secondary beam is propagated parallel to the sample surface, are involved in this multiple diffraction case. A RS interval of 3.3° around f = 0° position was measured while the electric field was increased up to 6 kV/cm. At this value, a phase transition was observed and the secondary peaks became narrower and changed their RS position indicating possible occurrence of a metastable ferroelectric phase
Disciplinas: Ingeniería
Palabras clave: Ingeniería eléctrica,
Rayos X,
Difracción,
Campo eléctrico,
Radiación sincrotrónica
Keyword: Engineering,
Electrical engineering,
X-rays,
Diffraction,
Electric field,
Synchrotron radiation
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