Preparation and characterization of nanostructured powders of hydroxyapatite



Título del documento: Preparation and characterization of nanostructured powders of hydroxyapatite
Revista: Superficies y vacío
Base de datos: PERIÓDICA
Número de sistema: 000355823
ISSN: 1665-3521
Autors: 1
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Institucions: 1Universidad Autónoma de San Luis Potosí, Facultad de Estomatología, San Luis Potosí. México
2Universidad Autónoma de San Luis Potosí, Facultad de Ingeniería, San Luis Potosí. México
3Universidad Autónoma de San Luis Potosí, Facultad de Ciencias, San Luis Potosí. México
4Centro de Investigación en Materiales Avanzados S.C., Parque de Investigación e Innovación Tecnológica, Apodaca, Nuevo León. México
Any:
Període: Jun
Volum: 25
Número: 2
País: México
Idioma: Inglés
Tipo de documento: Artículo
Enfoque: Experimental, aplicado
Resumen en inglés In this work, hydroxyapatite nanostructured powders were prepared with different crystallinity degree, crystal size and morphology using a simple aqueous precipitation method varying the pH and temperature parameters. We found that at higher pH values the crystal size grows and crystallinity was improved; at higher temperatures there is also a crystal size growth and crystallinity improving but this change is more significant, a change in the morphology of the nanopowders was also observed. Using XRD patterns and Rietveld analysis we found that the crystal size change from 9.15 to 26.4 nm. The prepared powders are highly agglomerated with a pseudo-spherical and rod-like morphology
Disciplines Ingeniería
Paraules clau: Ingeniería de materiales,
Biomateriales,
Hidroxiapatita,
Síntesis química,
Nanopolvo
Keyword: Engineering,
Materials engineering,
Biomaterials,
Hydroxyapatite,
Chemical synthesis,
Nanopowder
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