Preparation, optical characterization and stability of gold nanoparticles by facile methods



Título del documento: Preparation, optical characterization and stability of gold nanoparticles by facile methods
Revista: Revista mexicana de física
Base de datos: PERIÓDICA
Número de sistema: 000438971
ISSN: 0035-001X
Autors: 1
1
1
Institucions: 1Universidad Autónoma de Nuevo León, Facultad de Ciencias Químicas, San Nicolás de los Garza, Nuevo León. México
Any:
Període: Nov-Dic
Volum: 65
Número: 6
País: México
Idioma: Inglés
Tipo de documento: Artículo
Enfoque: Analítico, teórico
Resumen en inglés Gold nanoparticles were obtained by reduction of chloroauric acid HAuCl4 by two methods: conventional heating and microwave synthesis. In the microwave method, different cycles and sonication time were analyzed to establish the synthesis with smaller nanoparticle size and higher absorbance. The influence of synthesis method, cycles quantity and sonication time in the gold nanoparticles size and plasmon resonance were studied. Gold nanoparticles were analyzed by UV-Vis spectrophotometry, dynamic light scattering and surface electron microscopy. The results indicate that the nanoparticles obtained by microwave have bigger size than those obtained by conventional heating, however, present higher absorption. The microwave nanoparticles were analyzed one year after its synthesis and it was found that the plasmon resonance signal remains almost unchanged. Finally, two equations were derived from the analyzes for estimate molar extinction coefficient, molar concentration, and nanoparticle average diameter
Disciplines Física y astronomía
Paraules clau: Física atómica y molecular,
Síntesis,
Estabilidad,
Nanopartículas
Keyword: Atomic and molecular physics,
Synthesis,
Stability,
Nanoparticles
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