| Revista: | Ecletica quimica |
| Base de datos: | |
| Número de sistema: | 000552773 |
| ISSN: | 0100-4670 |
| Autors: | Ribeiro, Tatiana Gomes2 Franca, Juçara Ribeiro2 Marques, André Mesquita3 Coelho Kaplan, Maria Auxiliadora1 Faraco, André Augusto Gomes2 Castilho, Rachel Oliveira2 |
| Institucions: | 1UFRJ - Núcleo de Pesquisas de Produtos Naturais, Centro de Ciências da Saúde, Universidade Federal do Rio de Janeiro, Bloco H, Cidade Universitária, 21941-590 Rio de Janeiro – RJ., 2Universidade Federal de Minas Gerais, Faculdade de Farmácia, Belo Horizonte, Brasil., 3Universidade Federal do Rio de Janeiro, Núcleo de Pesquisas de Produtos Naturais, Centro de Ciências da Saúde, Rio de Janeiro, Brasil., |
| Any: | 2012 |
| Volum: | 37 |
| Número: | 1 |
| Paginació: | 61-67 |
| País: | Brasil |
| Idioma: | Inglés |
| Resumen en inglés | This work describes the development and validation of analytical method to assay nerolidol in a hydrophilic matrix of quitosan by UV/visible spectroscopy. The method is based on the formation of purple derivative between nerolidol and vanillin. The validated method was linear (2.5 - 50 mg mL-1, concentration range, r > 0.99), precise (RSD 0.44% for repeatability and 0.32% for intermediate precision), accurate (100.04% recovery), robust and specific. Detection and quantitation limits were 0.74 mg mL-1 and 2.26 mg mL-1, respectively. The method is simple and fast and it was applied successfully. Alternatively, the described method may be applied for the analysis of alcohols and unsaturated lipids. |
| Keyword: | Nnerolidol, Quitosan, Spectrometric method for alcohols and lipids |
| Text complet: | Texto completo (Ver PDF) |
